2 Jin Shu Pill Pharmacopoeia Standard 2. 1 Name Jin Shu Pill
ten thousand
2.2 Prescription Semen Strychni powder 1 15g, Herba Ephedrae 80g, Radix Angelicae Pubescentis 6g, Notopterygii Rhizoma 6g, Ramulus Cinnamomi 6g, Radix Glycyrrhizae 6g, Rhizoma homalomenae 6g, Achyranthis Radix 6g, Olibanum 6g (processed with vinegar), Fructus Chaenomelis 6g, Myrrha 6g (processed with vinegar), Radix Saposhnikoviae 6g, Eucommiae Cortex (processed with salt) 3g, and Fructus Lipuidambaris 6g.
2.3 For the preparation of the above fifteen herbs, except the powder of nux vomica, the other fourteen herbs, such as ephedra, are ground into fine powder, mixed with the powder of nux vomica and sieved. Add refined honey 150 ~ 170 g per 100g powder to make honeyed pills.
2.4 Characteristics This product is a brown honey pill; It tastes bitter.
2.5 Identification (1) Take 3g of this product, chop it up, moisten it with 2ml of concentrated ammonia solution, add 20ml of chloroform, ultrasonic for 30min, filter, evaporate the filtrate, and dissolve the residue with 2ml of chloroform as the test solution. In addition, chloroform was added to the reference substance of Warningen and the reference substance of brucine to prepare a mixed solution containing 65438±0mg per 65438±0ml as the reference substance solution. According to the test of thin-layer chromatography (Appendix ⅵ b of Pharmacopoeia Part I, 20 10), absorb the above two solutions 10μl, respectively spot them on the same silica gel G thin-layer plate, and use toluene-acetone-ethanol-concentrated ammonia solution (20: 25: 3: 2) as developing agent, unfold, take out, dry and spray. In the chromatogram of the test sample, spots with the same color appear in the position corresponding to the chromatogram of the control sample.
(2) Take ephedrine hydrochloride reference substance and add methanol to make a solution containing 0.5mg per kloc-0/ml as reference substance solution. According to the thin-layer chromatography test (Appendix ⅵ b of Pharmacopoeia I, 20 10), suck 10μl( 1) of the test solution under [Identification] and put them on the same silica gel G thin-layer plate respectively, and test the solution with cyclohexane-chloroform-ethanol-concentrated ammonia water (/kloc-0)
2.6 The inspection shall comply with the relevant provisions under Pills (Appendix of Pharmacopoeia 20 10/A).
2.7 the content was determined by high performance liquid chromatography (appendix ⅵ D of pharmacopoeia I, 20 10).
2.7. 1 chromatographic conditions and system applicability test, using octadecylsilane bonded silica gel as filler; Acetonitrile -0.0 1 mol/L sodium heptane sulfonate solution and 0.05mol/L potassium dihydrogen phosphate solution were used as mobile phases (adjusted to pH 2.8 with 10% phosphoric acid solution) (21:79); The detection wavelength is 254 nm. According to Ningfeng, the theoretical number of trays should not be less than 5000.
2.7.2 Preparation of reference solution Take an appropriate amount of strychnine reference substance, weigh it accurately, and add methanol to make a solution containing 60μg per kloc-0/ml.
2.7.3 Preparation of test solution Take this product with poor weight, cut it into pieces, mix it evenly, take about 65438±0.8g, weigh it accurately, put it in a conical flask with a stopper, add 3ml of water, shake it on an oscillator until it is completely dissolved, add 2ml of sodium hydroxide test solution, shake it evenly, add 50ml of methanol, and perform ultrasonic (power 400W, frequency 40kHz) for 20 minutes. Transfer the filtrate to a 100 ml volumetric flask, wash the residue with methanol and filter, combine the washing liquids into the same volumetric flask, add methanol to the scale, shake well, accurately measure 25ml, evaporate to dryness, dissolve the residue with methanol and transfer to a 100ml volumetric flask, add methanol to the scale, shake well, filter, and take the filtrate.
2.7.4 Determination method Accurately absorb 65,438+00μ l of control solution and test solution respectively, inject them into liquid chromatograph, and determine to obtain the product.
Each pill of this product contains 3.3 ~ 4.7 mg of nux vomica powder based on strychnine (C2 1H22N2O2).
2.8 Function indications: expelling wind and removing dampness, relaxing muscles and tendons and promoting blood circulation. Used for arthralgia due to wind-cold-dampness, numbness of limbs, pain of bones and muscles, and difficulty in walking.
2.9 Oral administration and dosage. Once 1 capsule, once a day 1 time.
2. 10 Pay attention to the taboos of pregnant women.
2. 1 1 specifications Each grain weighs 3g.
2. 12 storage seal.
2. 13 edition of China Pharmacopoeia 20 10 edition.
3 Pill standard issued by the Ministry of Traditional Chinese Medicine 3. 1 Pinyin name 10,000
3.2 standard number WS3B0 15289
3.3 Prescription Semen Strychni (processed) 80g Herba Ephedrae 80g Radix Angelicae Pubescentis 6g Radix Notopterygii 6g Ramulus Cinnamomi 6g Radix Glycyrrhizae 6g Rhizoma homalomenae 6g Radix Achyranthis Bidentatae 6g Olibanum (processed with vinegar) 6g Fructus Chaenomelis 6g Radix Saposhnikoviae 6g Eucommiae Cortex (processed with salt) 3g Radix Dipsaci 6g.
3.4 Make the above fifteen kinds of ingredients. Parch semen Strychni with sand, and pulverizing into fine pow. After the content of strychnine was determined by the content determination method of Semen Strychni (page), starch was used as diluent to adjust its content to 1. 15%. Pulverizing the rest 14 herbs such as Herba Ephedrae into fine powder, mixing with 80g of fine powder of Semen Strychni, grinding, mixing and sieving. Add refined honey 150~ 170g+070 g into every 100g powder to make honeyed pills.
3.5 Characteristics This product is a brown honey pill; It tastes bitter.
3.6 Identification (1) Take 3g of this product, chop it up, add 2ml of concentrated ammonia solution to wet the sample, add 20ml of chloroform, perform ultrasonic treatment for 30min, filter, evaporate the filtrate, and dissolve the residue with 2ml of chloroform as the test solution. In addition, chloroform was added to strychnine and brucine to prepare a mixed solution containing 1ml as a control solution. According to the thin-layer chromatography test (Appendix ⅵ b), absorb 65438 00μ l of the above two solutions, respectively spot them on the same silica gel G thin-layer plate with sodium carboxymethyl cellulose as adhesive, and use toluene acetone ethanol concentrated ammonia water test solution (4:5:0.6:0.4) as developing agent, unfold, take out, dry and spray diluted potassium bismuth iodide test solution. In the chromatogram of the test sample, spots with the same color appear in the position corresponding to the chromatogram of the control sample.
(2) Take ephedrine hydrochloride reference substance and add methanol to make a solution containing 0.5mg per kloc-0/ml as reference substance solution. According to the thin layer chromatography (appendix ⅵ b) test, absorption.
3.7 Identification (1): Take 10μ l of test solution and reference solution respectively, spread them on the same silica gel G thin-layer plate with sodium carboxymethyl cellulose as adhesive and chloroform-ethanol-cyclohexane concentrated ammonia solution (9:3:3:0.4) as developing agent, take them out, dry them, and spray them in/.
3.8 The inspection shall conform to the relevant regulations under Pills (Appendix 1A).
3.9 Functional indications: expelling wind and removing dampness, relaxing muscles and tendons and promoting blood circulation. Used for cold and wind, numbness of limbs, pain of bones and muscles, and difficulty in walking.
3. 10 Usage and dosage: take orally 1 pill once, once a day 1 time.
3. 1 1 Pay attention to pregnant women.
3. 12 specifications, each grain weighs 3g.
3. 13 Storage shall be sealed and moisture-proof.
4 pills "Wei family Tibetan prescription" Volume 8 4. 1 pill
4.2 Composition: Rhizoma Gastrodiae, Rhizoma Typhonii (processed), Radix Angelicae Sinensis (processed, soaked in wine), Radix Aconiti (processed, peeled navel), Fructus Chaenomelis, Radix Saposhnikoviae (processed), Scorpio (slightly soaked in ginger juice), Olibanum (processed) 1, and Myrrha.
4.3 Pills, as indicated in Volume VIII of Jia Zang Fang by Wei, are mainly used for treating blood deficiency and qi deficiency, rheumatism and arthralgia, muscle and bone discomfort, tight neck, inability to turn sideways and even earache.
4.4 Usage and dosage of Jin Shu Pills: 30 pills each time, and add to 50 pills. Black bean wine is always available.
4.5 The production method is fine powder, and the fermented batter is pills, which are as big as buttonwood.
5 Puji Fang 186 Jin Shu Pill 5. 1 Fangming Jin Shu Pill
5.2 consists of Cortex Erythrinae, Rhizoma Gastrodiae, Fructus Trichosanthis, Radix Saposhnikoviae, Tiger Bone, Achyranthis Radix, Lignum Aquilariae Resinatum 1.5, Radix Aucklandiae, Radix Angelicae Sinensis 1, Olibanum, Myrrha, Sanguis Draxonis, and melon seeds.
5.3 "Puji Fang", Volume 186, Jin Shu Pill is mainly used for tendons and arthralgia, which cannot be flexed or stretched.
5.4 Usage and dosage of Jin Shu Pills: Take 1 pill each time, chew slowly and take it with warm wine. If you don't take medicine, drink for half a minute first.
5.5 The preparation method is fine powder, and refined honey is pills, the size of which is like marbles.
5.6 Medication contraindications avoid hot things.
6 "Puji Fang" Volume 97 Jin Shu Pill 6. 1 Fangming Jin Shu Pill
6.2 It consists of two parts: Rhizoma Arisaematis (stir-fried), Semen Armeniacae Amarum (soup soaked, peeled Shuang Ren, brown with bran, not studied) 1, Fructus Gardeniae (stir-fried) 1, Radix Aconiti (stir-fried) 1, and natural copper (distilled liquor quenched).
6.3 Jin Shu Pill (Puji Fang, Volume 97) is mainly used for stroke, and it is difficult to carry out because of the acute muscles of hands and feet. A woman's blood is windy, but her hands and feet are twisted.
6.4 Usage and dosage of Jin Shu Pills: 765,438+00 pills each time, and 65,438+0 white spirit with white onion, twice a day. After 35 days, it will be effective if the body is moth-eaten, and the number of pills will increase if you don't sleep.
6.5 At the end of the production method, the researcher stirred it evenly, even using 2 ounces of walnut kernels to remove the yellow skin from the soup, grinding and stirring it evenly, and boiling the batter into balls with French wine, which are as big as buttonwood trees.
Jin Shu Pill was named Jin Shu Pill in the Selected Works of Traditional Chinese Medicine Prescriptions in Beijing 7. 1.
7.2 Radix Cyathulae 1 2, Radix Aucklandiae 1 2, Fructus Psoraleae (fried with salt) 5 yuan, Squama Manis (fried) 5 yuan, Cortex Eucommiae (fried) 5 yuan, Radix Rehmanniae, Radix Angelicae Dahuricae 5 yuan, Fructus Corni (fried) 1 2, Rhizoma Anemarrhenae 5 yuan and Alismatis/kloc-0. Magnolia officinalis (parched) 5 yuan, Uncaria 5 yuan, safflower 5 yuan, angelica 5 yuan, black bean 8liang, boat-fruited Sterculia 4liang, cassia twig 5 yuan, Notopterygium incisum 5 yuan, Radix Angelicae Pubescentis 5 yuan, Gentiana macrophylla 5 yuan, Rhizoma Cibotii (scalded) 1 2, Atractylodis Rhizoma (parched) 1 2.
7.3 Efficacy: Jin Shu Pill has the effects of relaxing tendons and activating collaterals, chasing wind and dispelling cold.
7.4 Jin Shu Pill indicated in Selected Prescriptions of Traditional Chinese Medicine in Beijing is mainly used for treating common cold, shoulder and back pain, lumbago and leg pain, numbness of limbs and difficulty in walking.
7.5 Usage and dosage of Jin Shu Pill: 1 pill, taken with warm boiled water twice a day.
7.6 The preparation method is fine powder, refined honey is pills, and each pill weighs 2 yuan.
8 Yangjia Tibetan Prescription Volume 4 Pill 8. 1 Pill
8.2 Ingredients: Angelica sinensis (washed and baked), kidney bean (raw), earthworm (peeled and fried), sweet melon seeds, papaya (peeled and cut and baked), clematis chinensis (peeled), Bai Jiao incense (researched separately), Rhizoma Drynariae (depilated), Erythrina bark (peeled), Lindera root, etc.
8.3 Indications: Jin Shu Pill, Volume IV of Yang Jia Zang Fang, indications: cold and dampness in meridians, swelling and pain in waist and feet, and inconvenient walking.
8.4 Usage and dosage of Jin Shu Pills: Take 1520 pills and take them with warm wine or salt soup twice a day before meals, 1.
8.5 The preparation method is fine powder, and the wine batter is pills as big as buttonwood.
9 Zhu Fang Ji 9. 1 Volume One Pill is called Pill.
9.2 Rhizoma Atractylodis (cut into pieces) 1, Radix Cyathulae (file with reed head removed) 1, Herba Cistanches (file) 1, Fructus Chaenomelis (pulp removed) 1 (soaked in wine 1 night, baked).
9.3 Efficacy Zhu's "Prescription Science" has the effect of nourishing yang and eliminating yin, expelling wind and removing dampness.
9.4 The pills contained in Volume I of Zhu Fang are suitable for people with hemiplegia and weakness of hands and feet caused by improper diet and daily life.
9.5 Usage and dosage of Jin Shu Pills: 5070 pills each time, taken with warm wine on an empty stomach, 1, twice a day. Take ten days, with light hands and feet and strong knees as the test.
9.6 The production method is fine powder, and the fermented batter is pills, which are as big as buttonwood.
9.7 taboo avoid mutton pig head.
10 The General Record of Shengji Volume VIII Jin Shu Pill 10. 1 Fangming Jin Shu Pill
10.2 is composed of aconite (peeled umbilical cord, half-fried) 1, Achyranthes bidentata (soaked in wine, cut into sections and baked) 1, earthworm (removed from soil, fried) 1, kidney bean 2 (raw flour) and Linderae (file) 6544.
10.3 Indications: Volume 8 Jin Shu Pills in Shengji Zonglu are mainly used for tendon apoplexy, limb contracture, no flexion and extension, and weakness of hands and feet.
10.4 Jin Shu pill usage and dosage: take 15 pill each time, and send salt soup regardless of time.
10.5 is made of powder, and refined honey is a pill, which is as big as a buttonwood.
Jin Shu Pill "Puji Fang" in ancient books: [Volume 97] Stroke limb contracture can't bend and stretch (attachment) 2) The upper part of carp nail (baked one or two) is the last part. Vinegar is displayed by hand and silk. Zaishujin Pill (published in General Record of Shengji) is used to treat tendon apoplexy. Don't bend or stretch limbs contracture. ...
Puji Fang: [Volume 186 Bimen] Jinbi (attached) Ben (except Miao Tu) and Daowei Pill are like Tongzida. After taking warm wine, you can't bend and stretch to 20 Jin Shu Pills. Pittosporum bark gastrodia elata. ...
"Compilation of Experience": "Compilation of Experience" Jia Sidao said: "This prescription has been used before and after, and it is very effective." Jin Shu Pill (suitable for men and women with inflexible hands and feet) in Zenggong Phlegm Record Olibanum Myrrha Angelica Rhizoma Drynariae (stir-fried) ...
"Standard of Syndrome Differentiation and Treatment: Class Prescriptions": [Volume 4] Five pieces of Bijiang ginger and two pieces of jujube are fried to seven points, and I am not allowed to take them at any time. Jin Shu pills can't bend and stretch muscles and bones. Cortex erythrinae, Myrrha, Sanguis Draxonis and Radix Aucklandiae (every two cents) ...
Complete works of ancient and modern medical systems: [Volume 11] Prescription Fangfeng Chuanxiong (equally divided) is covered with three slices of ginger in half water and decocted in seven parts. Jin Shu pills can't bend and stretch muscles and bones. Cortex erythrinae, Myrrha, Sanguis Draxonis and Radix Aucklandiae (every two cents) ...
Gushudo Jin Shu Pills
Jin Shu Pill Drug Instructions Jin Shu Ding Tong Wine Instructions (the second batch of instructions for the use of OTC proprietary Chinese medicines published by the State Drug Administration in 2002) Jin Shu Huoxue Ding Tong Powder Instructions (the second batch of instructions for the use of OTC proprietary Chinese medicines published by the State Drug Administration in 2002) Jin Shu Huoxue Liquor Instructions (the second batch of instructions for the use of OTC proprietary Chinese medicines published by the State Drug Administration in 2002). Instructions for Jin Shu rheumatism wine (OTC instruction model published by the US Food and Drug Administration in 2007) Instructions for Jin Shu Huoluo Pills (OTC instruction model published by the US Food and Drug Administration in 2007) Instructions for Jin Shu Ding Tong Tablets (OTC instruction model published by the US Food and Drug Administration in 2007) Instructions for Jin Shu decocted pills (published by the State Food and Drug Administration in 2007). Instructions for Shujin Jianluo Oil (OTC instruction model published by the State Food and Drug Administration in 2007) Instructions for Jin Shu Huoxue Ding Tong Powder (OTC instruction model revised by the State Food and Drug Administration of the United States on 20 10) Instructions for Jin Shu Huoluo Pill (the third batch of national OTC drug catalogue (I) variety instructions published by the State Drug Administration in 2003). Calculation and evaluation of body mass index index of human body surface area calculator safety period calculator expected date of delivery calculator Normal weight gain during pregnancy Drug safety classification (FDA) Five elements and eight characters Adult blood pressure evaluation Body temperature level evaluation Diabetes diet suggestion Clinical biochemical common unit conversion basal metabolic rate calculation Sodium supplement calculator Iron supplement calculator prescription common Latin abbreviations Quick check Pharmacokinetics common symbols Quick check Effective plasma osmotic pressure calculator Alcohol intake calculator.